Solid-phase microextraction as a green sample preparation strategy for volatile organic compound profiling in coffee: a review with AGREEprep-based evaluation

Yerkanat Syrgabek; Adrián Fuente-Ballesteros; Vânia G. Zuin Zeidler

doi:10.1038/s41538-026-00984-4

Solid-phase microextraction as a green sample preparation strategy for volatile organic compound profiling in coffee: a review with AGREEprep-based evaluation

Yerkanat Syrgabek
, Adrián Fuente-Ballesteros^*
, Vânia G. Zuin Zeidler^*

^*Corresponding author for this work

Al-Farabi Kazakh National University

Research output: Journal contributions › Scientific review articles › Research

1 Citation (Scopus)

Abstract

Solid-phase microextraction (SPME) is a solvent-free sample preparation technique increasingly applied in coffee analysis. This review examines recent studies (2020–2025) on SPME for volatile organic compound profiling in coffee. Coupled with GC-MS and chemometrics, SPME supports aroma characterization, authenticity evaluation, and sample classification. AGREEprep scores (0.29–0.73) suggest moderate greenness, highlighting SPME as a promising strategy with potential for greener and more sustainable coffee analysis. (Figure presented.)

Original language	English
Article number	235
Journal	npj Science of Food
Volume	10
Issue number	1
Number of pages	18
DOIs	https://doi.org/10.1038/s41538-026-00984-4
Publication status	Published - 12.2026

Bibliographical note

Publisher Copyright:
© The Author(s) 2026.

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 3 Good Health and Well-being
SDG 12 Responsible Consumption and Production

Research areas and keywords

Health sciences
Chemistry
Engineering
Environmental sciences

ASJC Scopus Subject Areas

Food Science
Public Health, Environmental and Occupational Health

Access to Document

10.1038/s41538-026-00984-4Licence: CC BY

Cite this

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title = "Solid-phase microextraction as a green sample preparation strategy for volatile organic compound profiling in coffee: a review with AGREEprep-based evaluation",

abstract = "Solid-phase microextraction (SPME) is a solvent-free sample preparation technique increasingly applied in coffee analysis. This review examines recent studies (2020–2025) on SPME for volatile organic compound profiling in coffee. Coupled with GC-MS and chemometrics, SPME supports aroma characterization, authenticity evaluation, and sample classification. AGREEprep scores (0.29–0.73) suggest moderate greenness, highlighting SPME as a promising strategy with potential for greener and more sustainable coffee analysis. (Figure presented.)",

keywords = "Health sciences, Chemistry, Engineering, Environmental sciences",

author = "Yerkanat Syrgabek and Adri{\'a}n Fuente-Ballesteros and \{Zuin Zeidler\}, \{V{\^a}nia G.\}",

note = "Publisher Copyright: {\textcopyright} The Author(s) 2026.",

year = "2026",

month = dec,

doi = "10.1038/s41538-026-00984-4",

language = "English",

volume = "10",

journal = "npj Science of Food",

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Solid-phase microextraction as a green sample preparation strategy for volatile organic compound profiling in coffee: a review with AGREEprep-based evaluation. / Syrgabek, Yerkanat; Fuente-Ballesteros, Adrián ; Zuin Zeidler, Vânia G.
In: npj Science of Food, Vol. 10, No. 1, 235, 12.2026.

Research output: Journal contributions › Scientific review articles › Research

TY - JOUR

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AU - Syrgabek, Yerkanat

AU - Fuente-Ballesteros, Adrián

AU - Zuin Zeidler, Vânia G.

PY - 2026/12

Y1 - 2026/12

N2 - Solid-phase microextraction (SPME) is a solvent-free sample preparation technique increasingly applied in coffee analysis. This review examines recent studies (2020–2025) on SPME for volatile organic compound profiling in coffee. Coupled with GC-MS and chemometrics, SPME supports aroma characterization, authenticity evaluation, and sample classification. AGREEprep scores (0.29–0.73) suggest moderate greenness, highlighting SPME as a promising strategy with potential for greener and more sustainable coffee analysis. (Figure presented.)

AB - Solid-phase microextraction (SPME) is a solvent-free sample preparation technique increasingly applied in coffee analysis. This review examines recent studies (2020–2025) on SPME for volatile organic compound profiling in coffee. Coupled with GC-MS and chemometrics, SPME supports aroma characterization, authenticity evaluation, and sample classification. AGREEprep scores (0.29–0.73) suggest moderate greenness, highlighting SPME as a promising strategy with potential for greener and more sustainable coffee analysis. (Figure presented.)

KW - Health sciences

KW - Chemistry

KW - Engineering

KW - Environmental sciences

UR - https://www.scopus.com/pages/publications/105046300632

U2 - 10.1038/s41538-026-00984-4

DO - 10.1038/s41538-026-00984-4

M3 - Scientific review articles

C2 - 42532984

AN - SCOPUS:105046300632

SN - 2396-8370

VL - 10

JO - npj Science of Food

JF - npj Science of Food

IS - 1

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ER -

Solid-phase microextraction as a green sample preparation strategy for volatile organic compound profiling in coffee: a review with AGREEprep-based evaluation

Abstract

Bibliographical note

UN SDGs

Research areas and keywords

ASJC Scopus Subject Areas

Access to Document

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Cite this